Read e-book online Solid-State NMR Spectroscopy of Inorganic Materials PDF

By John J. Fitzgerald (Eds.)

content material: Solid-state NMR spectroscopy of inorganic fabrics : an outline / John J. Fitzgerald and Susan M. DePaul --
Multiple-quantum magic-angle spinning NMR of half-integer quadrupolar nuclei / Ales Medek, Laura Marinelli, and Lucio Frydman --
Oxygen movement in uncomplicated and complicated oxides / Jeffrey A. Reimer and Stuart B. Adler --
The examine of fluoridated hydroxyapatite through ³¹P-¹⁹F rotational-echo, double-resonance NMR / Yong Pan --
Solid-state ¹H, ¹⁷O, and ²⁷Al NMR reports of the outside chemistry of alumina fabrics / John J. Fitzgerald --
an outline of solid-state NMR correlation experiments in phosphate glass platforms / R.M. Wenslow, ok. Fiske, and K.T. Mueller --
Borate glass constitution probed with dynamic attitude spinning NMR / J.W. Zwanziger, R.E. Youngman, and M. Braun --
A ¹⁷O sturdy kingdom NMR examine of the lead zirconium titanate method (PbZrxTi₁xO₃) / Walter G. Klemperer and David L. Richard --
Multinuclear NMR learn of host-guest interactions in sodalites / G. Engelhardt --
research of the host-guest buildings of molecular sieves by way of one- and two-dimensional solid-state NMR innovations / C.A. Fyfe, A.C. Diaz, A.R. Lewis, J.M. Chézeau, H. Grondey, and G.T. Kokotailo --
Double-resonance and two-dimensional silicon-29 NMR spectroscopy of minerals / Jay S. Shore, Susan M. DePaul, Matthias Ernst, and Brian L. Phillips --
Siloxane-based strong networks, from silicas to silicones / Gary E. Maciel --
Wide-line ¹⁴N NMR in solids / James P. Yesinowski and Edward A. Hill --
Solid-state NMR of nitrides and oxynitrides / M.E. Smith.

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Extra info for Solid-State NMR Spectroscopy of Inorganic Materials

Example text

M 19 4. Techniques for Distance Measurement between Heteronuclei (SEPOR* REDOR. 3, the strength of the heteronuclear dipolar coupling between two nuclei is given by ( / / ^ π ί γ ^ Γ ^ (η/2π). Thus, in systems which effectively contain isolated spin pairs, a measurement of the dipolar coupling constant translates into a direct determination of the interauclear distance. The Spin-Echo DOuble Resonance (SEDOR) technique (6) is the simplest method for measuring internuclear distances between a pair of unlike nuclei.

In the DAS technique, the sample is spun about one axis for part of the evolution period and then the sample is quickly reoriented and spun about a second axis relative to the static magnetic field (Figure 10B). The angles of the two axes and the amount of time spent at each angle are chosen such that the anisotropic evolution at the first angle (see last two terms in Equation (1)) is canceled out by the evolution at the second angle, leaving only the isotropic signal at the end (plus sidebands, if the spinning rate is not sufficiently rapid).

ACS Symposium Series; American Chemical Society: Washington, DC, 1999. Figure 16. 17 q 2 A two-dimensional 0 DAS spectrum of mineral coesite Si0 showing individual anisotropic quadrupolar powder patterns and corresponding simulations for each oxygen site (113). 292. 22° to 180°. ch001 (A) (Β) Figure 17. Two-dimensional exchange Li NMR spectra of the Li sites in Li Si0 at 33°C with mixing times (A) 47 ms and (B) 188 ms. The labels indicate exchange between selected pairs of Li0 Li0 , LiO , and Li0 sites.

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